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BS ISO 21330:2018

$142.49

Cigarettes. Determination of selected volatile organic compounds in the mainstream smoke of cigarettes. Method using GC/MS

Published By Publication Date Number of Pages
BSI 2018 26
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This document specifies a method for the quantification of selected volatile organic compounds (VOCs: 1,3-butadiene, isoprene, acrylonitrile, benzene and toluene) by GC-MS in mainstream cigarette smoke using ISO 3308 smoking parameters.

This method is applicable to cigarettes with nicotine-free dry particulate matter (NFDPM) yields between 1 mg/cigarette and 15 mg/cigarette.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Apparatus
10 6 Reagents
7 Preparation
7.1 Preparation of glassware
11 7.2 Preparation of standards
7.2.1 General
7.2.2 Preparation of internal standard spiking solution
7.2.3 Preparation of working standards for isoprene, acrylonitrile, benzene, and toluene
12 7.2.4 Preparation of working standards for 1,3-butadiene
13 8 Sampling
9 Tobacco product preparation
10 Sample generation — Smoking of cigarettes
10.1 General
14 10.2 Smoking machine setup
15 10.3 Smoking
10.3.1 General
10.3.2 Linear smoking
10.3.3 Rotary smoking
11 Sample analysis
11.1 Preparation of sample
16 11.2 Determination
11.2.1 GC-MS operating conditions
17 11.2.2 Calibration
11.2.3 Calculation
12 Repeatability and reproducibility
12.1 General
18 12.2 Results of the 2012 collaborative study
20 13 Test report
21 Annex A (informative) Examples of chromatograms
25 Bibliography
BS ISO 21330:2018
$142.49