BS EN ISO 9455-6:2022 2023
$142.49
Soft soldering fluxes. Test methods – Determination and detection of halide (excluding fluoride) content
Published By | Publication Date | Number of Pages |
BSI | 2023 | 24 |
This document specifies three quantitative methods for the determination of the ionic halide (excluding fluoride) content of soldering fluxes. Halides are calculated as chlorides. A useful qualitative test method for the detection of ionic halides is also described. Method A is a potentiometric titration method for the determination of halide (excluding fluoride) content and is applicable to flux classes 1 and 2, defined in ISO 9454-1. This method, which is considered the reference method for these fluxes, is suitable for halide contents generally within the range of 0,05 % mass fraction to 2 % mass fraction in the non-volatile matter of the flux. Method B is a titration method for the determination of the total halide (excluding fluoride) content of water-soluble fluxes. It is applicable to flux classes 2122 to 2124, 3112 to 3114 and 3212 to 3214, as defined in ISO 9454-1. Method C is a titration method for the determination of the halide (excluding fluoride) content of water-soluble fluxes containing phosphates and is applicable to flux class 331, as defined in ISO 9454-1. Method D is a qualitative test, using silver chromate test paper, for the presence of ionic halides. The technique can be used for all classes of flux.
PDF Catalog
PDF Pages | PDF Title |
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2 | undefined |
4 | European foreword Endorsement notice |
6 | Foreword |
7 | 1 āScope 2 āNormative references 3 āTerms and definitions 4 āMethod A: Potentiometric method (Reference method) 4.1 āPrinciple |
8 | 4.2 āReagents 4.3 āApparatus 4.4 āProcedure |
9 | 4.5 āCalculation of results 5 āMethod B: Titration method for halide (excluding fluoride) content of water-soluble fluxes 5.1 āPrinciple |
10 | 5.2 āReagents 5.3 āApparatus 5.4 āProcedure |
11 | 5.5 āStandardization of the ammonium thiocyanate solution (5.2.2) 5.6 āCalculation of results 6 āMethod C: Titration method for the determination of halide (excluding fluoride) content of water-soluble fluxes containing phosphates 6.1 āPrinciple |
12 | 6.2 āReagents 6.3 āApparatus 6.4 āProcedure |
13 | 6.5 āStandardization of the ammonium thiocyanate solution (6.2.2) 6.6 āCalculation of results 7 āMethod D: Qualitative test for the presence of ionic halides in flux 7.1 āPrinciple 7.2 āReagents |
14 | 7.3 āApparatus 7.4 āProcedure 7.4.1 āPreparation of flux test solution |
15 | 7.4.2 āTest procedure 8 āPrecision 8.1 āGeneral |
16 | 8.2 āMethod A 8.3 āMethod B 8.4 āMethod C 9 āTest report |
18 | Annex A (normative) Method for standardizing the silver nitrate solution |
21 | Bibliography |