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ASTM-E3 2011

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E3-11 Standard Guide for Preparation of Metallographic Specimens

Published By Publication Date Number of Pages
ASTM 2011 13
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ASTM E3-11

Historical Standard: Standard Guide for Preparation of Metallographic Specimens

ASTM E3

Scope

1.1 The primary objective of metallographic examinations is to reveal the constituents and structure of metals and their alloys by means of a light optical or scanning electron microscope. In special cases, the objective of the examination may require the development of less detail than in other cases but, under nearly all conditions, the proper selection and preparation of the specimen is of major importance. Because of the diversity in available equipment and the wide variety of problems encountered, the following text presents for the guidance of the metallographer only those practices which experience has shown are generally satisfactory; it cannot and does not describe the variations in technique required to solve individual specimen preparation problems.

Note 1—For a more extensive description of various metallographic techniques, refer to Samuels, L. E., Metallographic Polishing by Mechanical Methods, American Society for Metals (ASM) Metals Park, OH, 3rd Ed., 1982; Petzow, G., Metallographic Etching, ASM, 1978; and VanderVoort, G., Metallography: Principles and Practice, McGraw Hill, NY, 2nd Ed., 1999.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Keywords

alloys; grinding; metallography; metals; mounting; polishing; sectioning; specimen preparation (metallographic); Specimen preparation (for testing)–metals/alloys; Structural metals/alloys; Cleaning agents/processes; Electropolishing; Etching (materials/process); Grinding materials/operations; Inclusions–metals/alloys; Metallographic analysis/inspection; Metallurgical materials/applications; Metals and metallic materials–inclusion rating; Microscopic examination–metals/alloys; Mounting materials; Polishing; Sample preparation–metals/alloys; Sampling ferrous alloys

ICS Code

ICS Number Code 77.040.99 (Other methods of testing metals)

DOI: 10.1520/E0003-11

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
2 Significance and Use
Selection of Metallographic Specimens
Size of Metallographic Specimens
FIG. 1
3 Cutting of Metallographic Specimens
Cleanliness
Mounting of Specimens
TABLE 1
4 Plating of Specimens
TABLE 2
5 Grinding and Polishing
TABLE 3
TABLE 4
6 Special Procedures
TABLE 5
7 TABLE 6
TABLE 7
8 Keywords
X1. CLEANING SPECIMENS
X1.1
X1.2
X1.3
10 X2. PRESERVING PREPARED SPECIMENS
X2.1
X2.2
X2.3
TABLE X1.1
11 X3. APPLIED LOAD CONVERSIONS
X3.1
X3.2
X3.3
X3.4
X4. PROCEDURE IMPROVEMENT
X4.1
X4.2
X4.3
X4.4
X4.5
X4.6
X4.7
X4.8
X4.9
12 X4.10
X4.11
X4.12
X4.13
X4.14
X4.15
X4.16
13 REFERENCES
ASTM-E3 2011
$44.96