{"id":76273,"date":"2024-10-17T17:22:55","date_gmt":"2024-10-17T17:22:55","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/astm-e2866-2012\/"},"modified":"2024-10-24T19:26:06","modified_gmt":"2024-10-24T19:26:06","slug":"astm-e2866-2012","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/astm\/astm-e2866-2012\/","title":{"rendered":"ASTM-E2866 2012"},"content":{"rendered":"

ASTM E2866-12<\/h3>\n

Historical Standard: Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid<\/h4>\n
\n

ASTM E2866<\/h4>\n

Scope<\/strong><\/p>\n

1.1 This procedure covers the determination of Diisopropyl Methylphosphonate (DIMP), Ethyl Methylphosphonic Acid (EMPA), Isopropyl Methylphosphonic Acid (IMPA), Methylphosphonic Acid (MPA) and Pinacolyl Methylphosphonic Acid (PMPA), referred to collectively as organophosphonates (OPs) in this test method, in soil. This method is based upon solvent extraction of a soil by pressurized fluid extraction (PFE). The extract is filtered and analyzed by liquid chromatography\/tandem mass spectrometry (LC\/MS\/MS). OPs are qualitatively and quantitatively determined by this method.<\/p>\n

1.2 Units<\/span>\u2014<\/span>The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.<\/p>\n

1.3 The Method Detection Limit (MDL), electrospray ionization (ESI) mode and Reporting Range for the OPs are listed in Table 1.<\/p>\n

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.<\/span><\/p>\n

TABLE 1 Method Detection Limit and Reporting Range<\/p>\n

Keywords<\/strong><\/p>\n

liquid chromatography; mass spectrometry; organophosphonates; pressurized fluid extraction; soil<\/p>\n

ICS Code<\/strong><\/p>\n

ICS Number Code 13.080.10 (Chemical characteristics of soil)<\/p>\n

DOI:<\/strong> 10.1520\/E2866-12<\/p>\n<\/div>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
1<\/td>\nScope
Referenced Documents
TABLE 1 <\/td>\n<\/tr>\n
2<\/td>\nTerminology
Summary of Test Method
Significance and Use
Interferences <\/td>\n<\/tr>\n
3<\/td>\nApparatus
Reagents and Materials <\/td>\n<\/tr>\n
4<\/td>\nHazards
Glassware Washing, Sampling and Preservation
Preparation of LC\/MS\/MS
Calibration and Standardization
TABLE 2 <\/td>\n<\/tr>\n
5<\/td>\nTABLE 3 <\/td>\n<\/tr>\n
6<\/td>\nTABLE 4 <\/td>\n<\/tr>\n
7<\/td>\nTABLE 5 <\/td>\n<\/tr>\n
8<\/td>\nPressurized Fluid Extraction Procedure
TABLE 6 <\/td>\n<\/tr>\n
9<\/td>\nCalculation or Interpretation of Results
Report
Precision and Bias
Keywords <\/td>\n<\/tr>\n
10<\/td>\nTABLE 7
TABLE 8
TABLE 9 <\/td>\n<\/tr>\n
11<\/td>\nTABLE 10
TABLE 11
TABLE 12 <\/td>\n<\/tr>\n
12<\/td>\nTABLE 13
TABLE 14
TABLE 15 <\/td>\n<\/tr>\n
13<\/td>\nTABLE 16
TABLE 17
TABLE 18
TABLE 19 <\/td>\n<\/tr>\n
14<\/td>\nX1.
TABLE 20
TABLE 21
TABLE 22
TABLE X1.1 <\/td>\n<\/tr>\n
15<\/td>\nFIG. X1.1 <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

E2866-12 Standard Test Method for Determination of Diisopropyl Methylphosphonate, Ethyl Methylphosphonic Acid, Isopropyl Methylphosphonic Acid, Methylphosphonic Acid and Pinacolyl Methylphosphonic Acid in Soil by Pressurized Fluid Extraction and Analyzed by Liquid<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
ASTM<\/b><\/a><\/td>\n2012<\/td>\n15<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":76274,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[223,2637],"product_tag":[],"class_list":{"0":"post-76273","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-13-080-10","7":"product_cat-astm","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/76273","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/76274"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=76273"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=76273"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=76273"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}