{"id":451025,"date":"2024-10-20T09:15:32","date_gmt":"2024-10-20T09:15:32","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-178642023\/"},"modified":"2024-10-26T17:15:06","modified_gmt":"2024-10-26T17:15:06","slug":"bs-en-178642023","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-178642023\/","title":{"rendered":"BS EN 17864:2023"},"content":{"rendered":"
This document specifies a method for the determination of nitrogen content in IBDU (isobutylidenediurea) and CDU (crotonylidenediurea) using high-performance liquid chromatography (HPLC). The method is applicable to all fertilizers which do not contain interfering organic compounds.<\/p>\n
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2<\/td>\n | undefined <\/td>\n<\/tr>\n | ||||||
5<\/td>\n | European foreword <\/td>\n<\/tr>\n | ||||||
6<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle 5 Reagents 6 Apparatus and equipment <\/td>\n<\/tr>\n | ||||||
7<\/td>\n | 7 Sampling and sample preparation 8 Procedure 8.1 General 8.2 Calibration 8.2.1 Stock solution IBDU, mass concentration \u03c1(IBDU) = 100 mg\/l 8.2.2 Stock solution CDU, \u03c1(CDU) = 100 mg\/l 8.2.3 Calibration solutions <\/td>\n<\/tr>\n | ||||||
8<\/td>\n | Table 1 \u2014 Preparation of calibration solutions 8.3 Preparation of the test solution 8.4 Measurement 9 Calculation and expression of the result <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 10 Precision 10.1 Inter-laboratory tests 10.2 Repeatability 10.3 Reproducibility Table 2 \u2014 Mean values, repeatability and reproducibility limits 11 Test report <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | Annex A (informative) Results of the inter-laboratory tests Table A.1 \u2014 Statistical results of the inter-laboratory tests <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | Annex B (informative) Example chromatogram and calibration curves B.1 Example chromatogram Figure B.1 \u2014 Example chromatogram B.2 Example calibration curves <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | Figure B.2 \u2014 Example calibration curve CDU Figure B.3 \u2014 Example calibration curve IBDU <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | Annex C (informative) Example conditions for a suitable HPLC system <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" Inorganic fertilizers. Determination of nitrogen content in IBDU (isobutylidenediurea) and CDU (crotonylidenediurea)<\/b><\/p>\n |