{"id":291318,"date":"2024-10-19T19:46:50","date_gmt":"2024-10-19T19:46:50","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-iso-108102019\/"},"modified":"2024-10-25T16:48:35","modified_gmt":"2024-10-25T16:48:35","slug":"bs-iso-108102019","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-iso-108102019\/","title":{"rendered":"BS ISO 10810:2019"},"content":{"rendered":"

This document is intended to aid the operators of X-ray photoelectron spectrometers in their analysis of typical samples. It takes the operator through the analysis from the handling of the sample and the calibration and setting-up of the spectrometer to the acquisition of wide and narrow scans and also gives advice on quantification and on preparation of the final report.<\/p>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
2<\/td>\nNational foreword <\/td>\n<\/tr>\n
7<\/td>\nForeword <\/td>\n<\/tr>\n
8<\/td>\nIntroduction <\/td>\n<\/tr>\n
9<\/td>\n1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviations <\/td>\n<\/tr>\n
10<\/td>\n5 Overview of sample analysis <\/td>\n<\/tr>\n
12<\/td>\n6 Specimen characterization
6.1 General <\/td>\n<\/tr>\n
13<\/td>\n6.2 Specimen forms
6.2.1 General
6.2.2 Single crystal
6.2.3 Adsorbed or segregated layers, films and residues <\/td>\n<\/tr>\n
14<\/td>\n6.2.4 Interfaces and multilayered samples
6.2.5 Non-porous
6.2.6 Porous
6.2.7 Powder
6.2.8 Fibres and textiles
6.2.9 Internal interface
6.3 Material types
6.3.1 General
6.3.2 Metals and alloys <\/td>\n<\/tr>\n
15<\/td>\n6.3.3 Polymers
6.3.4 Semiconductors
6.3.5 Magnetic materials
6.3.6 Ceramics
6.3.7 Catalysts
6.3.8 Glass and insulators
6.3.9 Biological
6.3.10 Nanoparticles
6.4 Handling and mounting of specimens <\/td>\n<\/tr>\n
16<\/td>\n6.5 Specimen treatments
6.5.1 General
6.5.2 Heating and cooling
6.5.3 Scraping and fracture
6.5.4 Ion bombardment for analysing thin films
6.5.5 Exposure to gases and liquids
7 Instrument characterization[8]\u00a0
7.1 General <\/td>\n<\/tr>\n
17<\/td>\n7.2 Instrument checks
7.2.1 System health check[9]\u00a0
7.2.2 Mechanical
7.2.3 Sample holder
7.2.4 Vacuum <\/td>\n<\/tr>\n
18<\/td>\n7.3 Instrument calibration
7.3.1 Calibration of binding energy scale <\/td>\n<\/tr>\n
19<\/td>\n7.3.2 Intensity repeatability and intensity\/energy response function (IERF) <\/td>\n<\/tr>\n
20<\/td>\n7.3.3 Linearity of intensity scale test <\/td>\n<\/tr>\n
21<\/td>\n7.3.4 Lateral resolution
7.3.5 Depth resolution[21][22]\u00a0 <\/td>\n<\/tr>\n
24<\/td>\n7.3.6 Charge correction
7.4 Instrument set-up
7.4.1 Optimum settings <\/td>\n<\/tr>\n
25<\/td>\n7.4.2 System configuration
8 The wide-scan spectrum
8.1 Data acquisition
8.1.1 General <\/td>\n<\/tr>\n
26<\/td>\n8.1.2 Sample loading
8.1.3 Energy resolution
8.1.4 Energy range, step size and acquisition mode
8.1.5 X-ray source and conditions <\/td>\n<\/tr>\n
27<\/td>\n8.1.6 Charge correction
8.1.7 Spectrum acquisition
8.1.8 X-ray degradation
8.1.9 Thin surface layer
8.2 Data analysis
8.2.1 Calibration of the binding energy scale <\/td>\n<\/tr>\n
28<\/td>\n8.2.2 Peak table
8.2.3 Quantification <\/td>\n<\/tr>\n
29<\/td>\n8.2.4 \u200bAssessment of the composition employing the Tougaard extrinsic background[42] \u00a0
8.2.5 Requirement for narrow scans
9 The narrow scan
9.1 General
9.2 Data acquisition
9.2.1 Instrument settings
9.2.2 Choice of region <\/td>\n<\/tr>\n
30<\/td>\n9.3 Data analysis
9.3.1 Element identification
9.3.2 Chemical-state identification <\/td>\n<\/tr>\n
31<\/td>\n9.3.3 Quantification <\/td>\n<\/tr>\n
34<\/td>\n10 Test report <\/td>\n<\/tr>\n
36<\/td>\nBibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
BSI<\/b><\/a><\/td>\n2019<\/td>\n42<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":291321,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-291318","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/291318","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/291321"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=291318"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=291318"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=291318"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}